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Wednesday 5 September 2012

Preparation of Pentafluorinated Phenyl-Monohydro[60]fullerenes



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  https://www.thieme-connect.de/ejournals/abstract/10.1055/s-0032-1316578
 Wenli Shang et al
 Pentafluorinated phenyl-monohydro[60]fullerenes [C60(Arf)5H] are synthesized in good yields via reaction of the corresponding fluorinated phenyl copper reagent, itself prepared in situ from the fluorinated phenyl Grignard reagent (ArfMgBr) and copper(I) bromide-dimethyl sulfide complex, with [60]fullerene (C60) in 1,2-dichlorobenzene under a nitrogen atmosphere.
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