DR ANTHONY MELVIN CRASTO,WorldDrugTracker, helping millions, A 90 % paralysed man in action for you, I am suffering from transverse mylitis and bound to a wheel chair, With death on the horizon, nothing will not stop me except God
DR ANTHONY MELVIN CRASTO Ph.D ( ICT, Mumbai) , INDIA 30 Yrs Exp. in the feld of Organic Chemistry. Serving chemists around the world. Helping them with websites on Chemistry.Millions of hits on google, world acclamation from industry, academia, drug authorities for websites, blogs and educational contribution
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Friday 6 March 2015

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Sunday 1 March 2015

Synthesis of 2-phenyl indoxyls

Synthesis of 2-phenyl indoxyls 

ARKIVOC 2006 (xi) 37-46 pp. 37 - 46 



Synthesis of 2-phenylindoxyls
Michael C. Hewitt* and Liming Shao
Drug Discovery, Sepracor Inc., 84 Waterford Drive, Marlborough MA 01752, USA
E-mail: michael.hewitt@sepracor.com
http://www.arkat-usa.org/get-file/23564/


Michael HewittMichael hewitt



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10 a  n=1
10a: HPLC Rt = 9.87 min,

1 H NMR (400 MHz, CDCl3)
7.66-7.60 (m, 4H),
7.41-7.37 (m, 3H),
7.11-7.05 (m, 2H),
4.10-4.04 (m, 2H), NCH2
3.69-3.63 (m, 1H), 1H OF OCH2
3.58-3.51 (m, 1H); 1H OF OCH2


13C NMR (100 MHz, CDCl3) 197.2,C=0,  163.9, 137.8, 136.0, 128.9, 128.4, 126.5, 125.7, 122.8, 122.6, 114.8, 99.6, 67.9, 50.1;




http://www.nmrdb.org/13c/index.shtml?v=v2.14.1  PREDICT 13 C NMR

http://www.nmrdb.org/cosy/index.shtml?v=v2.14.1 COSY



GC-MS 13.4 min, M+ 251.

Selected gHMBC couplings (see above): 200 → 7.62, 7.64; 164 → 3.65, 3.5, 7.64; 99 → 3.65, 4.05.



1H NMR PREDICTION BELOW



Michael HewittMichael hewitt



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